NMR platform

The IPCM is the main user of several NMR spectrometers belonging to the NMR platform of the Federation FR2769. The NMR spectrometers presented below are located in the IPCM premises on the Jussieu campus.

These NMR spectrometers are analytical tools used daily by researchers for the follow-up of syntheses, routine characterization in molecular chemistry, or to perform more complex NMR studies on certain products.

400 MHz Bruker Nanobay: tower 42-43, 4th floor, room 407

Use: self-service for routine experiments during the day, and long experiments at night with the sample changer.

  • nanobay Avance III console
  • Operating software: Topspin 3.6
  • Probe: BBFO (direct probe, 1H, 13C, 31P, 11B,… and 19F, with automatic probe tuning + gradients)
  • Accessory: 60 position autosampler (BACS)
  • History: magnet installed in 2001, probe acquired in 2007, console installed in 2009, move in 2016, new computer in 2017

300 MHz Bruker Nanobay: tower 42-43, 4th floor, room 407

Use: self-service for routine experiments during the day, and long experiments at night with the sample changer.

  • nanobay Avance III console
  • Operating software: topspin 3.6
  • Probe: BBFO (direct probe, 1H, 13C, 31P, 11B,… and 19F, with automatic probe tuning + gradients)
  • Accessory: 60 position autosampler (BACS)
  • History: magnet and console installed in July 2010, moved in 2016

300 MHz Bruker Nanobay: tower 42-43, 4th floor, room 416

Use: self-service for routine experiments during the day, and long experiments at night with the sample changer.

  • nanobay Avance III console
  • Operating software: topspin 3.5
  • Probe: BBI (inverse probe, 1H, 13C + gradients)
  • Accessory: 16 position sample changer (Sample Xpress Lite)
  • History: console from 2010, installed on the 300 in 2015

300 MHz Advance II: tower 42-43, 4th floor, room 409

Use: manual, on reservation

  • Avance II console
  • Operating software: topspin 3.2
  • Probe park : 
    – QNP (direct probe, 1H, 13C, 31P, 19F+gradients)
    – QNP (direct probe, 1H, 13C, 31P, 19F)
    – BBO 5mm (direct broadband probe)
    – BBO 10mm (broadband direct probe)
    – BBI 5mm (inverse broadband probe with gradients)
    – Triple probe 1H, 31P and low γ-cores
  • Accessory: 60-position autosampler (BACS)
  • History: new computer in 2017

400 MHz Bruker-Jeol hybrid: tower 32-33, St. Bernard level

Use:lLong-term, temperature (heating only) or specific experiments. On booking

  • Console : ECZS400
  • Operating software: delta 6.1
  • Probe : 
    – Royal HFX (direct probe, 1H, 13C, 31P, 11B,… and 19F, with automatic probe tuning + gradients)
  • History: JEOL ECZS400 console installed in 2022, new BRUKER magnet installed in March 2011

600 MHz Bruker Avance III: tower 32-33, St. Bernard level

Use: long-term, temperature or specific experiments (use of sample changer possible)

  • Avance III console
  • Operating software: topspin 3.6
  • Probe park :  
    – BBFO (direct probe, 1H, 13C, 31P, 11B,… and 19F, with automatic probe tuning + gradients)
    – TXI (inverse probe 1.7mm, 1H, 13C and 15N, with automatic probe tuning + gradients)
    – BBO (10mm direct probe, 1H, and low &gamma cores, with automatic probe tuning + gradients),
    – 5mm triple inverse probe (1H, 31P and broadband + gradients)
  • Accessories: 24 position sample case, BCU05
  • History: magnet and console installed in March 2010, moved in 2016, Sample Case installation in 2017, new computer in 2018

Contact NMR platform for IPCM :

Claire TROUFFLARD

Engineer
(manager)

(phone 01 44 27 50 02)

Regina MARUCHENKO

Engineer

(phone 01 44 27 59 96)